Structure and function of flavivirus NS5 methyltransferase

J Virol. 2007 Apr;81(8):3891-903. doi: 10.1128/JVI.02704-06. Epub 2007 Jan 31.

Abstract

The plus-strand RNA genome of flavivirus contains a 5' terminal cap 1 structure (m7GpppAmG). The flaviviruses encode one methyltransferase, located at the N-terminal portion of the NS5 protein, to catalyze both guanine N-7 and ribose 2'-OH methylations during viral cap formation. Representative flavivirus methyltransferases from dengue, yellow fever, and West Nile virus (WNV) sequentially generate GpppA-->m7GpppA-->m7GpppAm. The 2'-O methylation can be uncoupled from the N-7 methylation, since m7GpppA-RNA can be readily methylated to m7GpppAm-RNA. Despite exhibiting two distinct methylation activities, the crystal structure of WNV methyltransferase at 2.8 A resolution showed a single binding site for S-adenosyl-L-methionine (SAM), the methyl donor. Therefore, substrate GpppA-RNA should be repositioned to accept the N-7 and 2'-O methyl groups from SAM during the sequential reactions. Electrostatic analysis of the WNV methyltransferase structure showed that, adjacent to the SAM-binding pocket, is a highly positively charged surface that could serve as an RNA binding site during cap methylations. Biochemical and mutagenesis analyses show that the N-7 and 2'-O cap methylations require distinct buffer conditions and different side chains within the K61-D146-K182-E218 motif, suggesting that the two reactions use different mechanisms. In the context of complete virus, defects in both methylations are lethal to WNV; however, viruses defective solely in 2'-O methylation are attenuated and can protect mice from later wild-type WNV challenge. The results demonstrate that the N-7 methylation activity is essential for the WNV life cycle and, thus, methyltransferase represents a novel target for flavivirus therapy.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Binding Sites
  • Crystallography, X-Ray
  • Dengue Virus / chemistry
  • Flavivirus
  • Methyltransferases / chemistry*
  • Methyltransferases / metabolism*
  • Mice
  • Mice, Inbred C3H
  • Models, Molecular
  • Molecular Sequence Data
  • Mutagenesis, Site-Directed
  • Protein Structure, Tertiary
  • RNA Caps / metabolism
  • RNA, Viral / metabolism
  • S-Adenosylmethionine / metabolism
  • Viral Nonstructural Proteins / chemistry*
  • Viral Nonstructural Proteins / metabolism*
  • Virulence Factors / chemistry
  • Virulence Factors / metabolism
  • West Nile Fever / virology
  • West Nile virus / chemistry*
  • West Nile virus / pathogenicity
  • West Nile virus / physiology*
  • Yellow fever virus / chemistry

Substances

  • NS5 protein, flavivirus
  • RNA Caps
  • RNA, Viral
  • Viral Nonstructural Proteins
  • Virulence Factors
  • S-Adenosylmethionine
  • Methyltransferases