Abstract
A process was optimized for the enzymatic synthesis of glyceryl ferulate with a yield of up to 96% using a vacuum-rotary evaporation strategy under following conditions: 15 mmol glycerol, 1.5 mmol ethyl ferulate, 170 mg Candida antarctica lipase, at 60 degrees C for 10 h and under a vacuum of 10 mm Hg. The immobilized lipase can be used 10 times.
MeSH terms
-
Chromatography, High Pressure Liquid
-
Coumaric Acids / chemistry
-
Coumaric Acids / metabolism*
-
Esterification
-
Fungal Proteins
-
Glycerol / chemistry*
-
Kinetics
-
Lipase / metabolism*
-
Molecular Structure
-
Solvents / chemistry*
-
Spectrometry, Mass, Electrospray Ionization
-
Temperature
Substances
-
Coumaric Acids
-
Fungal Proteins
-
Solvents
-
ferulic acid
-
Lipase
-
lipase B, Candida antarctica
-
Glycerol