Kinetics of the lipoperoxyl radical-scavenging activity of indicaxanthin in solution and unilamellar liposomes

Free Radic Res. 2007 Feb;41(2):226-33. doi: 10.1080/10715760601026614.

Abstract

The reaction of the phytochemical indicaxanthin with lipoperoxyl radicals generated in methyl linoleate methanol solution by 2,2'-azobis(2,4-dimethylvaleronitrile), and in aqueous soybean phosphatidylcholine unilamellar liposomes by 2,2'-azobis(2-amidinopropane)hydrochloride, was studied. The molecule acts as a chain-terminating lipoperoxyl radical scavenger in solution, with a calculated inhibition constant of 3.63 x 10(5) M(-1) s(-1), and a stoichiometric factor approaching 2. Indicaxanthin incorporated in liposomes prevented lipid oxidation, inducing clear-cut lag periods and decrease of the propagation rate. Both effects were concentration-dependent, but not linearly related to the phytochemical concentration. The consumption of indicaxanthin during liposome oxidation was remarkably delayed, the lower the concentration the longer the time-interval during which it remained in its native state. Indicaxanthin and alpha-tocopherol, simultaneously incorporated in liposomes, exhibited cooperative antioxidant effects and reciprocal protective interactions. The extent of synergism decreased at the increase of the ratio (indicaxanthin)/(alpha-tocopherol). A potential antioxidant mechanism of indicaxanthin is discussed in the context of the chemistry of the molecule, and of the possible reactivity of a short-lived intermediate.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • 1,2-Dipalmitoylphosphatidylcholine / metabolism
  • Amidines / pharmacology
  • Antioxidants / metabolism*
  • Antioxidants / pharmacology
  • Azo Compounds / pharmacology
  • Betaxanthins / metabolism*
  • Dose-Response Relationship, Drug
  • Drug Synergism
  • Free Radical Scavengers / metabolism*
  • In Vitro Techniques
  • Kinetics
  • Linoleic Acids / metabolism
  • Lipid Bilayers
  • Lipid Peroxidation
  • Lipid Peroxides / metabolism*
  • Liposomes / metabolism*
  • Methanol
  • Molecular Structure
  • Nitriles / pharmacology
  • Oxidation-Reduction
  • Phosphatidylcholines / metabolism
  • Pyridines / metabolism*
  • Solutions
  • Solvents
  • Suspensions
  • alpha-Tocopherol / metabolism
  • alpha-Tocopherol / pharmacology

Substances

  • Amidines
  • Antioxidants
  • Azo Compounds
  • Betaxanthins
  • Free Radical Scavengers
  • Linoleic Acids
  • Lipid Bilayers
  • Lipid Peroxides
  • Liposomes
  • Nitriles
  • Phosphatidylcholines
  • Pyridines
  • Solutions
  • Solvents
  • Suspensions
  • indicaxanthin
  • 2,2'-azobis(2,4-dimethylvaleronitrile)
  • methyl linoleate
  • 1,2-Dipalmitoylphosphatidylcholine
  • 2,2'-azobis(2-amidinopropane)
  • alpha-Tocopherol
  • Methanol