Determination of paroxetine in human saliva by reversed-phase high-performance liquid chromatography with UV detection

Nihon Shinkei Seishin Yakurigaku Zasshi. 2007 Feb;27(1):9-12.

Abstract

A rapid and sensitive high-performance liquid chromatographic method was validated and described for determination of paroxetine in human saliva. Following liquid-liquid extraction of the drug and an internal standard (dibucaine), chromatographic separation was accomplished using a C18 analytical column with a mobile phase consisting of 0.05 mol/L sodium phosphate buffer, pH 5.0, and acetonitrile (A 30:70, v/v; B 60:40, v/v). Paroxetine and the internal standard were detected by ultraviolet absorbance at 205 nm. The average recoveries of the drug and internal standard were 92.5% and 89%, respectively. The lower limits of detection and quantification were 1 and 4 ng/ml, respectively, and the calibration curve was linear over a concentration range of 4 ng/ml. The saliva level of paroxetine in patients with depression taking 10 to 40 mg/day of the drug was significantly correlated with the plasma level of paroxetine in each patient (r = 0.617, P < 0.004, n = 19). These data indicate that the saliva level of paroxetine could be a useful marker to predict the plasma level of the drug.

MeSH terms

  • Antidepressive Agents, Second-Generation / analysis*
  • Antidepressive Agents, Second-Generation / blood
  • Biomarkers / blood
  • Chromatography, High Pressure Liquid / methods*
  • Depression / drug therapy
  • Depression / metabolism
  • Drug Monitoring / methods*
  • Humans
  • Paroxetine / analysis*
  • Paroxetine / blood
  • Patient Compliance
  • Saliva / chemistry*

Substances

  • Antidepressive Agents, Second-Generation
  • Biomarkers
  • Paroxetine