Piezoelectric urea biosensor based on immobilization of urease onto nanoporous alumina membranes

Biosens Bioelectron. 2007 Jun 15;22(12):3283-7. doi: 10.1016/j.bios.2007.03.006. Epub 2007 Mar 14.

Abstract

The urease was immobilized onto nanoporous alumina membranes prepared by the two-step anodization method, and a novel piezoelectric urea sensing system with separated porous alumina/urease electrode has been developed through measuring the conductivity change of immobilized urease/urea reaction. The process of urease immobilization was optimized and the performance of the developed urea biosensor was evaluated. The obtained urea biosensor presented high-selectivity monitoring of urea, better reproducibility (S.D.=0.02, n=6), shorter response time (30s), wider linear range (0.5 microM to 3mM), lower detection limit (0.2 microM) and good long-term storage stability (with about 76% of the enzymatic activity retained after 30 days). The clinical analysis of the urea biosensor confirmed the feasibility of urea detection in urine samples.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aluminum Oxide / chemistry*
  • Biosensing Techniques / instrumentation*
  • Biosensing Techniques / methods
  • Enzymes, Immobilized / chemistry*
  • Hydrogen-Ion Concentration
  • Membranes, Artificial
  • Nanostructures
  • Porosity
  • Sensitivity and Specificity
  • Temperature
  • Urea / analysis*
  • Urease / chemistry*

Substances

  • Enzymes, Immobilized
  • Membranes, Artificial
  • Urea
  • Urease
  • Aluminum Oxide