Characterization of a subcomplex of mitochondrial NADH:ubiquinone oxidoreductase (complex I) lacking the flavoprotein part of the N-module

Biochim Biophys Acta. 2007 May;1767(5):393-400. doi: 10.1016/j.bbabio.2007.03.005. Epub 2007 Mar 15.

Abstract

Mitochondrial NADH:ubiquinone oxidoreductase is the largest and most complicated proton pump of the respiratory chain. Here we report the preparation and characterization of a subcomplex of complex I selectively lacking the flavoprotein part of the N-module. Removing the 51-kDa and the 24-kDa subunit resulted in loss of catalytic activity. The redox centers of the subcomplex could be reduced neither by NADH nor NADPH demonstrating that physiological electron input into complex I occurred exclusively via the N-module and that the NADPH binding site in the 39-kDa subunit and further potential nucleotide binding sites are isolated from the electron transfer pathway within the enzyme. Taking advantage of the selective removal of two of the eight iron-sulfur clusters of complex I and providing additional evidence by redox titration and site-directed mutagenesis, we could for the first time unambiguously assign cluster N1 of fungal complex I to mammalian cluster N1b.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Proteins / chemistry
  • Bacterial Proteins / genetics
  • Bacterial Proteins / metabolism
  • Catalysis
  • Electron Spin Resonance Spectroscopy
  • Electron Transport Complex I / chemistry*
  • Electron Transport Complex I / genetics
  • Electron Transport Complex I / metabolism
  • Flavin Mononucleotide / metabolism
  • Flavoproteins / genetics
  • Mutagenesis, Site-Directed
  • Sequence Deletion
  • Yersinia / enzymology*

Substances

  • Bacterial Proteins
  • Flavoproteins
  • Flavin Mononucleotide
  • Electron Transport Complex I