Characterization and structure of a Zn2+ and [2Fe-2S]-containing copper chaperone from Archaeoglobus fulgidus

J Biol Chem. 2007 Aug 31;282(35):25950-9. doi: 10.1074/jbc.M703311200. Epub 2007 Jul 3.

Abstract

Bacterial CopZ proteins deliver copper to P1B-type Cu+-ATPases that are homologous to the human Wilson and Menkes disease proteins. The genome of the hyperthermophile Archaeoglobus fulgidus encodes a putative CopZ copper chaperone that contains an unusual cysteine-rich N-terminal domain of 130 amino acids in addition to a C-terminal copper binding domain with a conserved CXXC motif. The N-terminal domain (CopZ-NT) is homologous to proteins found only in extremophiles and is the only such protein that is fused to a copper chaperone. Surprisingly, optical, electron paramagnetic resonance, and x-ray absorption spectroscopic data indicate the presence of a [2Fe-2S] cluster in CopZ-NT. The intact CopZ protein binds two copper ions, one in each domain. The 1.8 A resolution crystal structure of CopZ-NT reveals that the [2Fe-2S] cluster is housed within a novel fold and that the protein also binds a zinc ion at a four-cysteine site. CopZ can deliver Cu+ to the A. fulgidus CopA N-terminal metal binding domain and is capable of reducing Cu2+ to Cu+. This unique fusion of a redox-active domain with a CXXC-containing copper chaperone domain is relevant to the evolution of copper homeostatic mechanisms and suggests new models for copper trafficking.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Absorptiometry, Photon
  • Adenosine Triphosphatases / chemistry
  • Adenosine Triphosphatases / genetics
  • Adenosine Triphosphatases / metabolism
  • Amino Acid Motifs / physiology
  • Archaeal Proteins / chemistry*
  • Archaeal Proteins / genetics
  • Archaeal Proteins / metabolism
  • Archaeoglobus fulgidus / chemistry*
  • Archaeoglobus fulgidus / genetics
  • Archaeoglobus fulgidus / metabolism
  • Binding Sites / physiology
  • Cation Transport Proteins / chemistry
  • Cation Transport Proteins / genetics
  • Cation Transport Proteins / metabolism
  • Copper / chemistry*
  • Copper / metabolism
  • Copper-Transporting ATPases
  • Cysteine / chemistry
  • Cysteine / genetics
  • Cysteine / metabolism
  • Electron Spin Resonance Spectroscopy
  • Ion Transport / physiology
  • Iron / chemistry
  • Iron / metabolism
  • Metalloproteins / chemistry*
  • Metalloproteins / genetics
  • Metalloproteins / metabolism
  • Models, Molecular
  • Molecular Chaperones / chemistry*
  • Molecular Chaperones / genetics
  • Molecular Chaperones / metabolism
  • Oxidation-Reduction
  • Protein Binding / physiology
  • Protein Structure, Tertiary / physiology
  • Sequence Homology, Amino Acid
  • Structure-Activity Relationship
  • Zinc / chemistry*
  • Zinc / metabolism

Substances

  • Archaeal Proteins
  • Cation Transport Proteins
  • Metalloproteins
  • Molecular Chaperones
  • Copper
  • Iron
  • Adenosine Triphosphatases
  • Copper-Transporting ATPases
  • Zinc
  • Cysteine

Associated data

  • PDB/2HU9