Nongenomic actions of bile acids. Synthesis and preliminary characterization of 23- and 6,23-alkyl-substituted bile acid derivatives as selective modulators for the G-protein coupled receptor TGR5

J Med Chem. 2007 Sep 6;50(18):4265-8. doi: 10.1021/jm070633p. Epub 2007 Aug 9.

Abstract

23-Alkyl-substituted and 6,23-alkyl-disubstituted derivatives of chenodeoxycholic acid are identified as potent and selective agonists of TGR5, a G-protein coupled receptor for bile acids (BAs). In particular, we show that methylation at the C-23(S) position of natural BAs confers a marked selectivity for TGR5 over FXR, while the 6alpha-alkyl substitution increases the potency at both receptors. The present results allow for the first time a pharmacological differentiation of genomic versus nongenomic effects mediated by BA derivatives.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Bile Acids and Salts / chemical synthesis*
  • Bile Acids and Salts / chemistry
  • Bile Acids and Salts / pharmacology
  • CHO Cells
  • Cricetinae
  • Cricetulus
  • Crystallography, X-Ray
  • DNA-Binding Proteins / agonists
  • Humans
  • Ligands
  • Methylation
  • Models, Molecular
  • Molecular Structure
  • Receptors, Cytoplasmic and Nuclear / agonists
  • Receptors, G-Protein-Coupled / agonists*
  • Stereoisomerism
  • Structure-Activity Relationship
  • Transcription Factors / agonists
  • Ursodeoxycholic Acid / analogs & derivatives*
  • Ursodeoxycholic Acid / chemical synthesis
  • Ursodeoxycholic Acid / chemistry
  • Ursodeoxycholic Acid / pharmacology

Substances

  • 6-ethyl-23-methyl-3,7-dihydroxycholan-24-oic acid
  • Bile Acids and Salts
  • DNA-Binding Proteins
  • GPBAR1 protein, human
  • Ligands
  • Receptors, Cytoplasmic and Nuclear
  • Receptors, G-Protein-Coupled
  • Transcription Factors
  • farnesoid X-activated receptor
  • Ursodeoxycholic Acid