2'-epi-orobanchol and solanacol, two unique strigolactones, germination stimulants for root parasitic weeds, produced by tobacco

J Agric Food Chem. 2007 Oct 3;55(20):8067-72. doi: 10.1021/jf0715121. Epub 2007 Sep 6.

Abstract

Germination stimulants for root holoparasitic weeds broomrapes ( Orobanche and Phelipanche spp.) produced by tobacco ( Nicotiana tabacum L.) were purified and characterized. The root exudates of tobacco contained at least five different stimulants, and LC-MS/MS analyses revealed that four of them were strigolactones; a tetradehydrostrigol isomer, a didehydrostrigol isomer, and two strigol isomers. The two isomers of strigol were identified as (+)-orobanchol and its 2'-epimer by comparison of NMR and GC- and LC-MS data with those of synthetic standards. The structure of the tetradehydrostrigol isomer, the major stimulant of the bright yellow tobacco cultivars, was determined as 4-alpha-hydroxy-5,8-dimethyl-GR24 [( E)-4-alpha-hydroxy-5,8-dimethyl-3-(4-methyl-5-oxo-2,5-dihydrofuran-2-yloxy)methylene)-3a,4-dihydro-3 H-indeno[1,2- b]furan-2(8b H)-one] and named solanacol. 2'-Epi-orobanchol and solanacol are the first natural strigolactones having a 2'-epi stereochemistry and a benzene ring, respectively.

MeSH terms

  • Chromatography, Liquid
  • Germination / drug effects*
  • Lactones / analysis*
  • Lactones / chemistry
  • Lactones / pharmacology
  • Magnetic Resonance Spectroscopy
  • Mass Spectrometry
  • Nicotiana / chemistry*
  • Orobanche / growth & development*
  • Plant Roots / chemistry

Substances

  • (4-hydroxy-5,8-dimethyl-3-(4-methyl-5-oxo-2,5-dihydrofuran-2-yloxy)methylene)-3a,4-dihydro-3H-indeno(1,2-b)furan-2(8bH)-one
  • Lactones
  • orobanchol