Specific real-time PCR vs. fluorescent dyes for serum free DNA quantification

Clin Chem Lab Med. 2007;45(8):993-5. doi: 10.1515/CCLM.2007.191.

Abstract

Background: Detecting and quantifying circulating free DNA in patient serum has become a major challenge. New methods using conventional or automated DNA amplification have been developed. As quantitative real-time PCR (QPCR) remains expensive and requires dedicated automated instrumentation, we questioned whether simple quantification using fluorescent dyes is efficient for determination of free DNA levels in serum.

Methods: Serum samples from 180 cancer patients and 58 healthy volunteers were used for DNA quantification according to three methods: (i) using an exonic part of the beta-globin gene as the amplifying target; (ii) amplifying a 105-bp intron 1 part of the housekeeping cyclophilin A gene, both referring to specific standard curves; and (iii) using a PicoGreen DNA quantification kit without amplification.

Results: The 58 samples from healthy controls showed a reference limit of (95th percentile) <160 cyclophilin gene copies/mL. The 180 cancer samples displayed values ranging between 300 and 215,000 copies/mL. The cyclophilin method showed a high level of correlation with both the beta-globin (r=0.911, p<0.0001) and PicoGreen (r=0.915, p<0.0001) methods.

Conclusions: Aside from the disadvantage that the QPCR assays can only be used in clinical biochemistry laboratories that possess QPCR apparatus, the use of direct PicoGreen quantification displays major advantages in a routine context: it is less time-consuming and is quite inexpensive, but is still correlated with QPCR.

Publication types

  • Comparative Study
  • Evaluation Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adult
  • Aged
  • Case-Control Studies
  • Cyclophilins
  • DNA / analysis*
  • Fluorescent Dyes*
  • Globins
  • Humans
  • Middle Aged
  • Neoplasms / genetics
  • Polymerase Chain Reaction / methods*
  • Reagent Kits, Diagnostic / standards*

Substances

  • Fluorescent Dyes
  • Reagent Kits, Diagnostic
  • Globins
  • DNA
  • Cyclophilins