Consecutive palladium-catalyzed Hiyama-Heck reactions in aqueous media under ligand-free conditions

Chem Commun (Camb). 2007 Oct 21:(39):4056-8. doi: 10.1039/b707583a. Epub 2007 Jul 25.

Abstract

Symmetric and asymmetric (E)-1,2-diarylethenes are synthesized from aryl bromides by consecutive one-pot Hiyama-Heck reactions carried out in water and under air; the only additives required are sodium hydroxide, palladium acetate and poly(ethylene glycol), and the products are isolable in many cases by simple filtration of the water solution.