Cyclophilin A differentially activates monocytes and endothelial cells: role of purity, activity, and endotoxin contamination in commercial preparations

Atherosclerosis. 2008 Apr;197(2):564-71. doi: 10.1016/j.atherosclerosis.2007.08.025. Epub 2007 Oct 24.

Abstract

Background: Cyclophilin A (CyPA) is a cytoplasmic protein secreted under inflammatory conditions. Extracellular CyPA is detected in atherosclerotic plaques and has been observed to activate endothelial cells as well as monocytes.

Methods and results: Commercially available recombinant CyPA-induced expression of tissue factor (TF) and vascular cell adhesion molecule-1 (VCAM-1) in human aortic endothelial cells (HAEC). However, CyPA from commercial sources contained lipopolysaccharide at concentrations up to 18.9 ng/ml; moreover, it exhibited low purity as determined by protein spectrum analysis and low activity as assessed by peptidyl prolyl cis-trans isomerase (PPIase) assay. An in-house preparation of pure, active, and uncontaminated CyPA failed to induce endothelial TF or VCAM-1 expression; moreover, it was not chemotactic for HAEC. In contrast, such CyPA exhibited potent chemotactic activity on monocytic THP-1 cells, with a maximal effect on migration occurring at a concentration of 5.5 x 10(-9)mol/l. Pretreatment of CyPA with cyclosporine A prevented its effect on THP-1 cell migration; similarly, PPIase-deficient mutant CyPA protein did not induce migration of these cells. In-house prepared CyPA induced the release of Il-6, but not TNF-alpha, from THP-1 cells.

Conclusions: Commercially available CyPA exhibits low purity and activity and may be contaminated by endotoxin. Pure, active, and uncontaminated CyPA does not induce endothelial TF or VCAM-1 expression; instead, it acts as a potent monocyte chemoattractant and induces monocyte Il-6 release, implying a role for extracellular CyPA in the pathogenesis of atherosclerosis via activation of monocytes rather than endothelial cells.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aorta / cytology
  • Cells, Cultured
  • Chemotactic Factors / physiology
  • Cyclophilin A / biosynthesis
  • Cyclophilin A / chemistry*
  • Cyclophilin A / physiology*
  • Drug Contamination*
  • Endothelial Cells / drug effects
  • Endothelial Cells / physiology*
  • Humans
  • Lipopolysaccharides / isolation & purification
  • Lipopolysaccharides / pharmacology
  • Monocytes / drug effects
  • Monocytes / physiology*
  • Thromboplastin / metabolism
  • Vascular Cell Adhesion Molecule-1 / metabolism

Substances

  • Chemotactic Factors
  • Lipopolysaccharides
  • Vascular Cell Adhesion Molecule-1
  • Thromboplastin
  • Cyclophilin A