In vitro cyclooxygenase-2 protein expression and enzymatic activity in neoplastic cells

J Vet Intern Med. 2007 Sep-Oct;21(5):1048-55. doi: 10.1892/0891-6640(2007)21[1048:ivcpea]2.0.co;2.

Abstract

Background: Cyclooxygenase-2 (COX-2) and its principle enzymatic metabolite, prostaglandin E2 (PGE2), are implicated in cancer progression. Based upon immunohistochemical (IHC) evidence that several tumor types in animals overexpress COX-2 protein, COX-2 inhibitors are used as anticancer agents in dogs and cats.

Hypothesis: IHC is inaccurate for assessing tumor-associated COX-2 protein and enzymatic activity.

Methods: Five mammalian cell lines were assessed for COX-2 protein expression by IHC and Western blot analysis (WB), and functional COX-2 activity was based upon PGE2 production.

Results: Detection of COX-2 protein by IHC and WB were in agreement in 4 of 5 cell lines. In 1 cell line that lacked COX-2 gene transcription because of promoter hypermethylation (HCT-116), IHC produced false-positive staining for COX-2 protein expression. Functional COX-2 enzymatic activity was dissociated from relative IHC-based COX-2 protein expression in 2 cell lines (RPMI 2650 and SCCF1). The RPMI 2650 cell line demonstrated strong COX-2 protein expression but minimal PGE2 production.

Conclusions and clinical importance: Western blot is more accurate than IHC for the detection of COX-2 protein in the cell lines studied. Furthermore, the semiquantitative identification of COX-2 protein by IHC or WB does not necessarily correlate with enzymatic activity. Based upon the potential inaccuracy of IHC and dissociation of COX-2 protein expression from enzymatic activity, the practice of instituting treatment of tumors with COX-2 inhibitors based solely on IHC results should be reconsidered.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Blotting, Western / veterinary
  • Cat Diseases / enzymology*
  • Cat Diseases / genetics
  • Cat Diseases / pathology
  • Cats
  • Cell Line, Tumor
  • Cyclooxygenase 2 / biosynthesis*
  • Cyclooxygenase 2 / genetics
  • Cyclooxygenase 2 / metabolism
  • Dinoprostone / analysis
  • Dog Diseases / enzymology*
  • Dog Diseases / genetics
  • Dog Diseases / pathology
  • Dogs
  • HCT116 Cells
  • Humans
  • Immunohistochemistry / veterinary
  • Mice
  • Neoplasms / enzymology*
  • Neoplasms / genetics
  • Neoplasms / pathology
  • Neoplasms / veterinary*
  • Phosphorylation
  • RNA, Neoplasm / chemistry
  • RNA, Neoplasm / genetics
  • Reverse Transcriptase Polymerase Chain Reaction / veterinary
  • Sequence Analysis, DNA

Substances

  • RNA, Neoplasm
  • Cyclooxygenase 2
  • Dinoprostone