Synthesis of diiodo butadiynyl-bridged bisphthalocyaninatozinc(II) complexes

J Inorg Biochem. 2008 Mar;102(3):388-94. doi: 10.1016/j.jinorgbio.2007.10.025. Epub 2007 Nov 28.

Abstract

Two functionalized phthalocyanine-based chromophore systems having two iodophthalocyaninatozinc(II) rings bound together through a butadiynyl linkage 1a,b have been synthesized by oxidative Eglinton coupling of the corresponding monomer, and fully characterized. The electronic characteristics of these extensively linearly pi-conjugated compounds were modulated by the introduction of different peripheral substituents into the phthalocyanine moieties and investigated by UV-visible spectroscopy. The reactivity of the two iodo substituents was explored to prepare a novel bisphthalocyanine containing two ethynylphenyl moieties, thus pointing out the possibility of incorporating other electro and/or photoactive moieties in the BisPc system, taking advantage of the iodo-functionalization.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Indoles / chemistry*
  • Isoindoles
  • Molecular Structure
  • Organometallic Compounds / chemical synthesis*
  • Organometallic Compounds / chemistry*
  • Spectrophotometry, Ultraviolet

Substances

  • Indoles
  • Isoindoles
  • Organometallic Compounds
  • phthalocyanine