Cyclopropanecarboxylic acid esters as potential prodrugs with enhanced hydrolytic stability

Org Lett. 2008 Feb 7;10(3):509-11. doi: 10.1021/ol702892e. Epub 2008 Jan 9.

Abstract

Esters of cyclopropanecarboxylic acid demonstrate a substantial increase in stability under both acid- and base-catalyzed hydrolytic conditions. Comparison of the stability of valacyclovir 13 with the cyclopropane analogue 14 shows that at 40 degrees C and pH 6 the half-life of 14 is >300 h while the value for 13 is 69.7 h. CBS-QB3 calculations on isodesmic reactions for transfer of groups from an alkane to an ester show that a cyclopropyl group provides hyperconjugative stabilization.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Acyclovir / analogs & derivatives*
  • Acyclovir / chemistry
  • Acyclovir / pharmacology
  • Antiviral Agents / chemistry*
  • Antiviral Agents / pharmacology
  • Cyclopropanes / chemistry*
  • Cyclopropanes / pharmacology
  • Esters
  • Hydrolysis
  • Molecular Structure
  • Prodrugs / chemistry*
  • Prodrugs / pharmacology
  • Valacyclovir
  • Valine / analogs & derivatives*
  • Valine / chemistry
  • Valine / pharmacology

Substances

  • Antiviral Agents
  • Cyclopropanes
  • Esters
  • Prodrugs
  • cyclopropanecarboxylic acid
  • cyclopropane
  • Valine
  • Valacyclovir
  • Acyclovir