Raman spectroscopy and X-ray diffraction studies of stress effects in PbTiO3 thin films

IEEE Trans Ultrason Ferroelectr Freq Control. 2007 Dec;54(12):2623-31. doi: 10.1109/TUFFC.2007.589.

Abstract

A systematic study of domain structure and residual stress evolution with film thickness and of phase transition in c/a epitaxial PbTiO(3)/LaAlO(3) films using X-ray diffraction and Raman spectroscopy is reported. Both techniques revealed that the films are under tensile residual stress in the film plane and that a-domains are more stressed than c-domains. The two components of the large A(1)(TO) Ramanmodes are associated with a- and c-domains and their intensity ratio correlates to the volume fraction of a-domains. The evolution of the Raman signature with temperature revealed that the spectrum of a-domains disappears around 480 degrees C, whereas c-domains present an anomaly in their spectrum at 500 degrees C but maintain a well-defined Raman signature up to 600 degrees C.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Computer Simulation
  • Elasticity
  • Lead / chemistry*
  • Materials Testing
  • Membranes, Artificial*
  • Models, Chemical*
  • Models, Molecular*
  • Molecular Conformation
  • Spectrum Analysis, Raman*
  • Stress, Mechanical
  • Titanium / chemistry*
  • X-Ray Diffraction*

Substances

  • Membranes, Artificial
  • lead titanate
  • Lead
  • Titanium