Automated gain control ion funnel trap for orthogonal time-of-flight mass spectrometry

Anal Chem. 2008 Jul 15;80(14):5367-76. doi: 10.1021/ac8003488. Epub 2008 May 31.

Abstract

Time-of-flight mass spectrometry (TOF MS) is increasingly used in proteomics research. Herein, we report on the development and characterization of a TOF MS instrument with improved sensitivity equipped with an electrodynamic ion funnel trap (IFT) that employs an automated gain control (AGC) capability. The IFT-TOF MS was coupled to a reversed-phase capillary liquid chromatography (RPLC) separation and evaluated in experiments with complex proteolytic digests. When applied to a global tryptic digest of Shewanella oneidensis proteins, an order-of-magnitude increase in sensitivity compared to that of the conventional continuous mode of operation was achieved due to efficient ion accumulation prior to TOF MS analysis. As a result of this sensitivity improvement and related improvement in mass measurement accuracy, the number of unique peptides identified in the AGC-IFT mode was 5-fold greater than that obtained in the continuous mode.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Automation
  • Ions / chemistry
  • Mass Spectrometry / instrumentation*
  • Mass Spectrometry / methods*
  • Peptides / chemistry
  • Time Factors

Substances

  • Ions
  • Peptides