Detection of myosin light chain phosphorylation--a cell-based assay for screening Rho-kinase inhibitors

Biochem Biophys Res Commun. 2008 Sep 19;374(2):356-60. doi: 10.1016/j.bbrc.2008.07.028. Epub 2008 Jul 16.

Abstract

Here, we describe the first example of a cell-based myosin light chain phosphorylation assay in 96-well format that allows for the rapid screening of novel Rho-kinase inhibitors. We obtained IC(50) values for the prototypic Rho-kinase inhibitors Y-27632 (1.2+/-0.05microM) and Fasudil (3.7+/-1.2microM) that were similar to those previously published utilizing electrophoresis-based methodologies. H-1152P, a Fasudil analog showed an IC(50) value of 77+/-30nM. Data derived from a set of 21 novel Rho-kinase inhibitors correlate with those generated by a well-established cell-based phenotypic Rho-kinase inhibition assay (R(2)=0.744). These results show that imaging technology measuring changes in myosin light chain phosphorylation can be used to rapidly generate quantitative IC(50) values and to screen a larger set of small molecule Rho-kinase inhibitors and suggests that this approach can be broadly applied to other cell lines and signaling pathways.

MeSH terms

  • Amides / pharmacology
  • Animals
  • Cell Line
  • Drug Evaluation, Preclinical / methods*
  • Myosin Light Chains / analysis*
  • Phosphoproteins / analysis*
  • Phosphorylation / drug effects
  • Protein Kinase Inhibitors / isolation & purification*
  • Protein Kinase Inhibitors / pharmacology
  • Pyridines / pharmacology
  • rho-Associated Kinases / antagonists & inhibitors*

Substances

  • Amides
  • Myosin Light Chains
  • Phosphoproteins
  • Protein Kinase Inhibitors
  • Pyridines
  • Y 27632
  • rho-Associated Kinases