Absolute stereochemistry of amphidinolide Q

Org Lett. 2008 Sep 4;10(17):3709-11. doi: 10.1021/ol8013123. Epub 2008 Aug 5.

Abstract

The absolute configurations at five chiral centers in amphidinolide Q (1), a cytotoxic 12-membered macrolide isolated from a marine dinoflagellate Amphidinium sp., were elucidated to be 4R, 7R, 9S, 11R, and 13R on the basis of NMR analyses and a modified Mosher's method.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Dinoflagellida / chemistry
  • Macrolides / chemistry*
  • Models, Molecular
  • Molecular Conformation
  • Nuclear Magnetic Resonance, Biomolecular / methods
  • Stereoisomerism

Substances

  • Macrolides
  • amphidinolide Q