1 Department of Inorganic and Physical Chemistry, Centre for Ordered Materials, Organometallics and Catalysis (COMOC), University of Ghent, Krijgslaan 281, building S3, 9000 Ghent, Belgium. [email protected]
Spectroscopic evidence of the thermally induced generation of multifunctional mesoporous materials through metamorphism within the pore walls of ethenylene-bridged PMOs is presented.