Crystallization and preliminary X-ray diffraction analysis of the complex between a human anti-interferon antibody fragment and human interferon alpha-2A

Acta Crystallogr Sect F Struct Biol Cryst Commun. 2009 Jan 1;65(Pt 1):14-6. doi: 10.1107/S1744309108037925. Epub 2008 Dec 25.

Abstract

Recombinant human interferon alpha-2A (rhIFN-alpha-2A) has been crystallized in complex with the recombinantly produced Fab fragment of a therapeutic monoclonal antibody (MEDI545; IgG1/kappa) which targets several human interferon alpha subtypes. This constitutes the first reported crystals of a human type I interferon bound to an antibody. The orthorhombic crystals belonged to either space group I222 or I2(1)2(1)2(1), with unit-cell parameters a = 134.82, b = 153.26, c = 163.49 A. The diffraction of the crystals extended to 3.0 A resolution. The asymmetric unit contained two Fab-rhIFN-alpha-2A complexes. This corresponded to a crystal volume per protein weight (V(M)) of 3.02 A(3) Da(-1) and a solvent content of 59.3%. The corresponding three-dimensional structure is expected to shed light on the mechanism of action of MEDI545 and the molecular basis of its specificity.

MeSH terms

  • Antibodies, Anti-Idiotypic / chemistry*
  • Antibodies, Monoclonal / chemistry
  • Crystallization
  • Electrophoresis, Polyacrylamide Gel
  • Humans
  • Imaging, Three-Dimensional
  • Immunoglobulin Fab Fragments / chemistry
  • Interferon alpha-2
  • Interferon-alpha / chemistry*
  • Interferons / chemistry*
  • Molecular Conformation
  • Molecular Structure
  • Recombinant Proteins
  • X-Ray Diffraction

Substances

  • Antibodies, Anti-Idiotypic
  • Antibodies, Monoclonal
  • Immunoglobulin Fab Fragments
  • Interferon alpha-2
  • Interferon-alpha
  • Recombinant Proteins
  • Interferons