Inter- and intra-individual variations of urinary endogenous metabolites in healthy male college students using (1)H NMR spectroscopy

Clin Chem Lab Med. 2009;47(2):188-94. doi: 10.1515/CCLM.2009.040.

Abstract

Background: Most human metabolomics studies have shown that spectral outputs of (1)H nuclear magnetic resonance fingerprinting are strongly influenced by inter- and intra-individual variations; however, few studies have been performed to evaluate the inter- and intra-individual variations in urinary endogenous metabolites.

Methods: We recruited 30 male college students to evaluate the factors affecting intra- and inter-individual variations in urinary endogenous metabolites. Statistical analysis for variations in urinary metabolites was performed after eliminating outliers found in principal component analysis (PCA) plots.

Results: Inter-individual variations were relatively low for 2-oxoglutarate, succinate, citrate, dimethylglycine, and taurine, but high for trimethylaminoxide (TMAO), hippurate, and lactate. Intra-individual variations for 2-oxoglutarate, citrate, dimethylglycine, and taurine were relatively low, but high for TMAO and hippurate. The factors affecting inter-individual variation of lactate were age, body mass index, beverages, and alcohol, whereas the factors affecting intra-individual variation of lactate were age and fish. Kim Chi intake affected the inter-individual variation of succinate, citrate, TMAO, and hippurate; however, it did not affect the intra-individual variation of endogenous metabolites.

Conclusions: Our results showed that inter- and intra-individual variations in urinary endogenous metabolites were very large, and significant factors affecting inter- and intra-individual variation were diverse, even after eliminating outliers in PCA analysis.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adult
  • Analysis of Variance
  • Carboxylic Acids / urine*
  • Health*
  • Humans
  • Ketoglutaric Acids / urine*
  • Magnetic Resonance Spectroscopy
  • Male
  • Methylamines / urine*
  • Principal Component Analysis*
  • Protons
  • Reproducibility of Results
  • Sarcosine / analogs & derivatives*
  • Sarcosine / urine
  • Sensitivity and Specificity
  • Taurine / urine*

Substances

  • Carboxylic Acids
  • Ketoglutaric Acids
  • Methylamines
  • Protons
  • Taurine
  • dimethylglycine
  • Sarcosine