Protein tyrosine phosphatase 1B inhibitory by dammaranes from Vietnamese Giao-Co-Lam tea

J Ethnopharmacol. 2009 Jul 15;124(2):240-5. doi: 10.1016/j.jep.2009.04.027. Epub 2009 May 3.

Abstract

Ethnopharmacological relevance: Gynostemma pentaphyllum (Thunb.) tea was used in Vietnamese folk medicine as anti-diabetic agent.

Aim of the study: This study was aimed to investigate the inhibitory activities of fractions and constituents isolated from Gynostemma pentaphyllum on protein tyrosine phosphatase 1B (PTP1B) since it has been proposed as a treatment therapy for type 2 diabetes and obesity.

Materials and methods: The 70% EtOH extract, CHCl3 fraction, EtOAc fraction, BuOH fraction, and seven isolated dammarane triterpenes were evaluated for their inhibitory activity in protein phosphatase enzymes (PTP1B and VHR).

Results: CHCl3-soluble fraction showed a dose-dependent inhibitory activity of the PTP1B enzyme with the IC50 value of 30.5 microg/mL. Among seven tested compounds, compounds 6 showed the most potent PTP1B inhibitory activity with IC50 value of 5.3+/-0.4 microM compared to a range 15.7-28.5 microM for the other six compounds. The inhibition mode of 6 was competitive toward p-NPP with a K(i) value of 2.8 microM.

Conclusion: These study results suggested that the PTP1B inhibitory activity of these dammaranes may enable this plant to play an important role in the treatment of diabetes.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Dammaranes
  • Diabetes Mellitus, Type 2 / drug therapy
  • Dose-Response Relationship, Drug
  • Gynostemma / chemistry*
  • Humans
  • Inhibitory Concentration 50
  • Medicine, East Asian Traditional
  • Nitrophenols / metabolism
  • Organophosphorus Compounds / metabolism
  • Phytotherapy
  • Plant Components, Aerial
  • Plant Extracts / chemistry
  • Plant Extracts / pharmacology*
  • Protein Tyrosine Phosphatase, Non-Receptor Type 1 / antagonists & inhibitors*
  • Triterpenes / isolation & purification
  • Triterpenes / pharmacology*

Substances

  • Nitrophenols
  • Organophosphorus Compounds
  • Plant Extracts
  • Triterpenes
  • nitrophenylphosphate
  • Protein Tyrosine Phosphatase, Non-Receptor Type 1