Solubility of Epiphany endodontic sealer prepared with resinous solvent

J Endod. 2009 May;35(5):715-8. doi: 10.1016/j.joen.2009.01.021.

Abstract

Purpose: To evaluate in vitro the solubility of the Epiphany endodontic filling material Epiphany (Pentron Clinical Technologies, Wallingford, CT) prepared with its resinous solvent.

Methods: The specimens were prepared in the following experimental conditions: (1) GI, epiphany without photoactivation; (2) GII, Epiphany prepared with resinous solvent without photoactivation; (3) GIII, Epiphany followed by photoactivation; and (4) GIV, Epiphany prepared with resinous solvent followed by photoactivation. Ten specimens of each group were obtained from Teflon molds with 80% reduction in volume of the specimen's dimensions based on American National Standard Institute/American Dental Association (ANSI/ADA) Specification No. 57. The samples were weighted and immersed in distilled water for 7 days. After this period, they were removed, dried, and weighed again. Solubility was calculated by using samples weight loss (%). The immersion liquid was evaluated through atomic absorption spectrometry.

Results: The sealers without photoactivation were statistically similar (p > 0.05) between themselves (GI = 6.93% and GII = 6.39%) and different from the uncured sealers, which were statistically different between themselves (p < 0.05) (GIII = 3.56% and GIV = 0.47%). Only the Epiphany sealer prepared with resinous solvent followed by photoactivation presented solubility values within ANSI/ADA requirements, liberating the following amounts of ions: 114.43 microg of Ca(2+)/mL, 2.4 microg of Mg(2+)/mL, 0.33 microg of Fe(2+)/mL, 0.11 microg of Zn(2+)/mL, 1.31 microg of Ni(2+)/mL, and 7.1 microg of Na(+)/mL.

Conclusion: The association of resinous solvent to the Epiphany sealer followed by photoactivation resulted in a filling material with low solubility and expressive liberation of calcium ions.

MeSH terms

  • Calcium / analysis
  • Humans
  • Immersion
  • Iron / analysis
  • Light
  • Magnesium / analysis
  • Materials Testing
  • Methacrylates / chemistry
  • Methacrylates / radiation effects
  • Nickel / analysis
  • Resins, Synthetic / chemistry
  • Resins, Synthetic / radiation effects
  • Root Canal Filling Materials / chemistry*
  • Root Canal Filling Materials / radiation effects
  • Sodium / analysis
  • Solubility
  • Solvents / chemistry*
  • Spectrophotometry, Atomic
  • Time Factors
  • Water / chemistry
  • Zinc / analysis

Substances

  • Methacrylates
  • Resins, Synthetic
  • Root Canal Filling Materials
  • Solvents
  • epiphany sealer
  • Water
  • ethoxylated bis-phenol A dimethacrylate
  • Nickel
  • Sodium
  • Iron
  • Magnesium
  • Zinc
  • Calcium