Racemic calcium tartrate tetrahydrate [form (II)] in rat urinary stones

Acta Crystallogr B. 2009 Jun;65(Pt 3):350-4. doi: 10.1107/S0108768109013688. Epub 2009 May 19.

Abstract

The title compound, [Ca(C4H4O6)].4H2O, calcium tartrate tetrahydrate, is a new triclinic centrosymmetric form identified in rat kidney calculus. The crystal structure was determined from powder and single-crystal X-ray diffraction. The four water molecules belong to one square face of the Ca-atom coordination (a square antiprism), the four O atoms of the second square face coming from two tartrate anions, building infinite chains alternating Ca atom polyhedra and tartrate anions along a, with the chains cross-linked by a network of hydrogen bonds.

MeSH terms

  • Animals
  • Crystallization
  • Crystallography, X-Ray
  • Hydrogen Bonding
  • Isomerism
  • Male
  • Microscopy, Electron, Scanning
  • Models, Molecular
  • Molecular Conformation
  • Rats
  • Rats, Wistar
  • Tartrates / chemistry*
  • Urinary Calculi / chemistry*
  • Urinary Calculi / ultrastructure

Substances

  • Tartrates
  • tartaric acid