Characterization and synthetic application of a novel beta1,3-galactosyltransferase from Escherichia coli O55:H7

Bioorg Med Chem. 2009 Jul 15;17(14):4910-5. doi: 10.1016/j.bmc.2009.06.005. Epub 2009 Jun 9.

Abstract

A beta1,3-galactosyltransferase (WbgO) was identified in Escherichia coli O55:H7. Its function was confirmed by radioactive activity assay and structure analysis of the disaccharide synthesized with the recombinant enzyme. WbgO requires a divalent metal ion, either Mn(2+) or Mg(2+), for its activity and is active between pH 6.0-8.0 with a pH optimum of 7.0. N-acetylglucosamine (GlcNAc) and oligosaccharides with GlcNAc at the non-reducing end were shown to be its preferred substrates and it can be used for the synthesis of type 1 glycan chains from these substrates. Together with a recombinant bacterial GlcNAc-transferase, benzyl beta-lacto-N-tetraoside was synthesized with the purified WbgO to demonstrate the synthetic utility of WbgO.

MeSH terms

  • Acetylglucosamine / metabolism*
  • Amino Acid Sequence
  • Bacterial Proteins / genetics
  • Bacterial Proteins / metabolism
  • Escherichia coli / enzymology*
  • Escherichia coli / genetics
  • Galactosyltransferases / analysis*
  • Galactosyltransferases / genetics
  • Galactosyltransferases / isolation & purification
  • Galactosyltransferases / metabolism*
  • Magnesium / metabolism
  • Manganese / metabolism
  • Molecular Sequence Data
  • N-Acetylglucosaminyltransferases / genetics
  • N-Acetylglucosaminyltransferases / metabolism
  • Oligosaccharides / chemical synthesis
  • Oligosaccharides / chemistry
  • Oligosaccharides / metabolism*
  • Recombinant Proteins / analysis
  • Recombinant Proteins / genetics
  • Recombinant Proteins / isolation & purification
  • Recombinant Proteins / metabolism
  • Sequence Alignment
  • Substrate Specificity

Substances

  • Bacterial Proteins
  • Oligosaccharides
  • Recombinant Proteins
  • Manganese
  • lacto-N-neotetraose
  • WbgO protein, E coli
  • Galactosyltransferases
  • N-Acetylglucosaminyltransferases
  • Magnesium
  • Acetylglucosamine