Synthesis and evaluation of 5-benzylidene(thio)barbiturate-beta-D-glycosides as mushroom tyrosinase inhibitors

Bioorg Med Chem Lett. 2009 Aug 1;19(15):4055-8. doi: 10.1016/j.bmcl.2009.06.018. Epub 2009 Jun 13.

Abstract

A series of 5-benzylidene(thio)barbiturate-beta-d-glycosides were designed, synthesized and evaluated as a new class of mushroom tyrosinase inhibitors. The results demonstrated that most of compounds had more potent inhibitory activities than arbutin (IC(50) 8.4mmol/L). Compound 12b was found to be the most potent inhibitor with IC(50) value of 0.05mmol/L. SARs analysis suggested that (1) 5-benzylidenethiobarbiturate substructures were efficacious for the inhibitory activity; (2) the lipophilic property of acetylated sugar moiety facilitated the inhibitory potency; (3) the hydroxyl group of 3'-configuration contributed to the increase of inhibitory effects. In addition, the inhibition mechanism study revealed that 5-benzylidene(thio)barbiturate-beta-d-glycosides were irreversible inhibitors.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Agaricales / drug effects*
  • Agaricales / enzymology*
  • Animals
  • Chemistry, Pharmaceutical / methods
  • Drug Design
  • Enzyme Inhibitors / chemical synthesis
  • Enzyme Inhibitors / pharmacology
  • Glycosides / chemical synthesis*
  • Glycosides / pharmacology
  • Inhibitory Concentration 50
  • Levodopa / chemistry
  • Mice
  • Models, Chemical
  • Monophenol Monooxygenase / antagonists & inhibitors*
  • Monophenol Monooxygenase / chemistry
  • Peptides / chemical synthesis*
  • Peptides / pharmacology
  • Structure-Activity Relationship

Substances

  • Enzyme Inhibitors
  • Glycosides
  • Peptides
  • Levodopa
  • Monophenol Monooxygenase