{4-[(Carbamimidoylhydrazono)methyl-kappa2N1,N4]-5-hydroxymethyl-2-methylpyridinium-3-olate-kappaO}(methanol-kappaO)copper(II) dinitrate

Acta Crystallogr C. 2009 Sep;65(Pt 9):m337-9. doi: 10.1107/S0108270109029023. Epub 2009 Aug 8.

Abstract

The title compound, [Cu(C(9)H(13)N(5)O(2))(CH(4)O)](NO(3))(2), consists of square-planar cationic complex units where the Cu(II) centre is coordinated by an N,N',O-tridentate pyridoxal-aminoguanidine Schiff base adduct and a methanol molecule. The tridentate ligand is a zwitterion exhibiting an almost planar conformation. The dihedral angles between the mean planes of the pyridoxal ring and the six- and five-membered chelate rings are all less than 2.0 degrees. The charge on the complex cation is neutralized by two nitrate counter-ions. Extensive N-H...O and C-H...O hydrogen bonding connects these ionic species and leads to the formation of layers. The pyridoxal hydroxy groups are the only fragments that deviate significantly from the flat layer structure; these groups are involved in O-H...O hydrogen bonding, connecting the layers into a three-dimensional crystal structure.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Copper / chemistry*
  • Crystallography, X-Ray
  • Hydrogen Bonding
  • Models, Molecular
  • Organometallic Compounds / chemistry*
  • Schiff Bases / chemistry*

Substances

  • Organometallic Compounds
  • Schiff Bases
  • Copper