Dissociation of calmodulin-target peptide complexes by the lipid mediator sphingosylphosphorylcholine: implications in calcium signaling

J Biol Chem. 2010 Jan 15;285(3):1799-808. doi: 10.1074/jbc.M109.053116. Epub 2009 Nov 12.

Abstract

Previously we have identified the lipid mediator sphingosylphosphorylcholine (SPC) as the first potentially endogenous inhibitor of the ubiquitous Ca2+ sensor calmodulin (CaM) (Kovacs, E., and Liliom, K. (2008) Biochem. J. 410, 427-437). Here we give mechanistic insight into CaM inhibition by SPC, based on fluorescence stopped-flow studies with the model CaM-binding domain melittin. We demonstrate that both the peptide and SPC micelles bind to CaM in a rapid and reversible manner with comparable affinities. Furthermore, we present kinetic evidence that both species compete for the same target site on CaM, and thus SPC can be considered as a competitive inhibitor of CaM-target peptide interactions. We also show that SPC disrupts the complex of CaM and the CaM-binding domain of ryanodine receptor type 1, inositol 1,4,5-trisphosphate receptor type 1, and the plasma membrane Ca2+ pump. By interfering with these interactions, thus inhibiting the negative feedback that CaM has on Ca2+ signaling, we hypothesize that SPC could lead to Ca2+ mobilization in vivo. Hence, we suggest that the action of the sphingolipid on CaM might explain the previously recognized phenomenon that SPC liberates Ca2+ from intracellular stores. Moreover, we demonstrate that unlike traditional synthetic CaM inhibitors, SPC disrupts the complex between not only the Ca2+-saturated but also the apo form of the protein and the target peptide, suggesting a completely novel regulation for target proteins that constitutively bind CaM, such as ryanodine receptors.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Apoproteins / metabolism
  • Binding, Competitive
  • Calcium / metabolism
  • Calcium Signaling / drug effects*
  • Calmodulin / antagonists & inhibitors*
  • Calmodulin / chemistry
  • Calmodulin / metabolism*
  • Cattle
  • Humans
  • Intracellular Space / drug effects
  • Intracellular Space / metabolism
  • Kinetics
  • Melitten / chemistry
  • Melitten / metabolism
  • Micelles
  • Molecular Sequence Data
  • Phosphorylcholine / analogs & derivatives*
  • Phosphorylcholine / metabolism
  • Phosphorylcholine / pharmacology
  • Protein Structure, Tertiary
  • Ryanodine Receptor Calcium Release Channel / chemistry
  • Ryanodine Receptor Calcium Release Channel / metabolism
  • Spectrometry, Fluorescence
  • Sphingosine / analogs & derivatives*
  • Sphingosine / metabolism
  • Sphingosine / pharmacology

Substances

  • Apoproteins
  • Calmodulin
  • Micelles
  • Ryanodine Receptor Calcium Release Channel
  • sphingosine phosphorylcholine
  • Phosphorylcholine
  • Melitten
  • Sphingosine
  • Calcium