Specificity of the BRISC deubiquitinating enzyme is not due to selective binding to Lys63-linked polyubiquitin

J Biol Chem. 2010 Apr 2;285(14):10344-52. doi: 10.1074/jbc.M109.059667. Epub 2009 Dec 23.

Abstract

BRISC (Brcc36-containing isopeptidase complex) is a four-subunit deubiquitinating (DUB) enzyme that has a catalytic subunit, called Brcc36, that is a member of the JAMM/MPN(+) family of zinc metalloproteases. A notable feature of BRISC is its high specificity for cleaving Lys(63)-linked polyubiquitin. Here, we show that BRISC selectivity is not due to preferential binding to Lys(63)-linked polyubiquitin but is instead dictated by how the substrate isopeptide linkage is oriented within the enzyme active site. BRISC possesses a high affinity binding site for the ubiquitin hydrophobic surface patch that accounts for the bulk of the affinity between enzyme and substrate. Although BRISC can interact with either subunit of a diubiquitin conjugate, substrate cleavage occurs only when BRISC is bound to the hydrophobic patch of the distal (i.e. the "S1") ubiquitin at a ubiquitin-ubiquitin cleavage site. The importance of the Lys(63)-linked proximal (S1') ubiquitin was underscored by our finding that BRISC could not cleave the isopeptide bond joining a ubiquitin to a non-ubiquitin substrate. Finally, we also show that Abro1, another BRISC subunit, binds directly to Brcc36 and that the Brcc36-Abro1 heterodimer includes a minimal complex with Lys(63)-specific DUB activity.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Binding Sites
  • Carbon-Nitrogen Lyases / metabolism
  • Catalytic Domain
  • Deubiquitinating Enzymes
  • HeLa Cells
  • Humans
  • Lysine / metabolism*
  • Membrane Proteins / metabolism*
  • Multiprotein Complexes / genetics
  • Multiprotein Complexes / metabolism*
  • Polyubiquitin / metabolism*
  • Proteasome Endopeptidase Complex / metabolism*
  • Protein Binding
  • Recombinant Proteins / genetics
  • Recombinant Proteins / isolation & purification
  • Recombinant Proteins / metabolism
  • Substrate Specificity
  • Trans-Activators / metabolism
  • Ubiquitination
  • Ubiquitins / metabolism*

Substances

  • Membrane Proteins
  • Multiprotein Complexes
  • PSMD14 protein, human
  • Recombinant Proteins
  • Trans-Activators
  • Ubiquitins
  • diubiquitin conjugate
  • Polyubiquitin
  • BRCC3 protein, human
  • Deubiquitinating Enzymes
  • Proteasome Endopeptidase Complex
  • Carbon-Nitrogen Lyases
  • isopeptidase
  • Lysine