Synthesis and complete assignment of the 1H and 13C NMR signals of new acetamido and aminoflavonoid derivatives

Gilles Casano; Maxime Robin; Pascale Barbier; Vincent Peyrot; Robert Faure

doi:10.1002/mrc.2638

Synthesis and complete assignment of the 1H and 13C NMR signals of new acetamido and aminoflavonoid derivatives

Magn Reson Chem. 2010 Sep;48(9):738-44. doi: 10.1002/mrc.2638.

Authors

Gilles Casano¹, Maxime Robin, Pascale Barbier, Vincent Peyrot, Robert Faure

Affiliation

¹ UMR 6263, ISM2, Université Paul Cézanne, Case 552 Avenue Escadrille Normandie-Niemen, 13397 Marseille Cedex 20, France.

PMID: 20589726
DOI: 10.1002/mrc.2638

Abstract

The complete (1)H and (13)C NMR assignment of 9 acetamidochalcones, 18 acetamidoflavones, 18 aminoflavones, 9 acetamidoflavonols and 9 aminoflavonols has been performed using one- and two-dimensional NMR techniques including COSY, HMQC and HMBC experiments.

2010 John Wiley & Sons, Ltd.

MeSH terms

Acetamides / chemical synthesis*
Acetamides / chemistry*
Carbon Isotopes
Flavonoids / chemical synthesis*
Flavonoids / chemistry*
Magnetic Resonance Spectroscopy / standards
Molecular Structure
Protons
Reference Standards
Stereoisomerism

Substances

Acetamides
Carbon Isotopes
Flavonoids
Protons