Aziridinomitosanes via lactam cyclization

Org Lett. 2010 Sep 17;12(18):4030-3. doi: 10.1021/ol101595u.

Abstract

Aziridinomitosane ketones 4 and 24 are accessed by internal acyl anion equivalent-lactam cyclization of 29 in a convergent route. The key aziridinolactam 6 is prepared by tin-lithium exchange via the lithiated aziridine 11.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Aziridines / chemistry*
  • Catalysis
  • Cyclization
  • Mitomycins / chemistry*
  • Molecular Structure
  • Stereoisomerism

Substances

  • Aziridines
  • Mitomycins
  • mitosane
  • aziridine