One-pot microwave-assisted protocol for the synthesis of substituted 2-amino-1H-imidazoles

Mol Divers. 2011 May;15(2):491-6. doi: 10.1007/s11030-010-9270-5. Epub 2010 Aug 26.

Abstract

An efficient microwave-assisted one-pot two-step protocol was developed for the construction of disubstituted 2-amino-1H-imidazoles. This process involves the sequential formation of 2,3-dihydro-2-hydroxyimidazo[1,2-a]pyrimidinium salts from readily available 2-aminopyrimidines and α-bromoketones, followed by cleavage of the pyrimidine ring with hydrazine.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Catalysis / radiation effects*
  • Chemistry / methods*
  • Hot Temperature
  • Imidazoles / chemical synthesis*
  • Microwaves*
  • Pyrimidines / chemistry

Substances

  • Imidazoles
  • Pyrimidines
  • 2-aminopyrimidine
  • 2-aminoimidazole