Hpy188I-DNA pre- and post-cleavage complexes--snapshots of the GIY-YIG nuclease mediated catalysis

Nucleic Acids Res. 2011 Mar;39(4):1554-64. doi: 10.1093/nar/gkq821. Epub 2010 Oct 8.

Abstract

The GIY-YIG nuclease domain is present in all kingdoms of life and has diverse functions. It is found in the eukaryotic flap endonuclease and Holliday junction resolvase Slx1-Slx4, the prokaryotic nucleotide excision repair proteins UvrC and Cho, and in proteins of 'selfish' genetic elements. Here we present the structures of the ternary pre- and post-cleavage complexes of the type II GIY-YIG restriction endonuclease Hpy188I with DNA and a surrogate or catalytic metal ion, respectively. Our structures suggest that GIY-YIG nucleases catalyze DNA hydrolysis by a single substitution reaction. They are consistent with a previous proposal that a tyrosine residue (which we expect to occur in its phenolate form) acts as a general base for the attacking water molecule. In contrast to the earlier proposal, our data identify the general base with the GIY and not the YIG tyrosine. A conserved glutamate residue (Glu149 provided in trans in Hpy188I) anchors a single metal cation in the active site. This metal ion contacts the phosphate proS oxygen atom and the leaving group 3'-oxygen atom, presumably to facilitate its departure. Taken together, our data reveal striking analogy in the absence of homology between GIY-YIG and ββα-Me nucleases.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Base Sequence
  • Biocatalysis
  • Catalytic Domain
  • Crystallography, X-Ray
  • Cysteine / chemistry
  • DNA / chemistry*
  • DNA Cleavage
  • Deoxyribonucleases, Type II Site-Specific / chemistry*
  • Models, Molecular
  • Molecular Sequence Data
  • Protein Folding

Substances

  • DNA
  • endodeoxyribonuclease Hpy188I
  • Deoxyribonucleases, Type II Site-Specific
  • Cysteine

Associated data

  • PDB/3OQG
  • PDB/3OR3