Design, synthesis, and biological activity of novel 5-((arylfuran/1H-pyrrol-2-yl)methylene)-2-thioxo-3-(3-(trifluoromethyl)phenyl)thiazolidin-4-ones as HIV-1 fusion inhibitors targeting gp41

J Med Chem. 2011 Jan 27;54(2):572-9. doi: 10.1021/jm101014v. Epub 2010 Dec 29.

Abstract

On the basis of our earlier molecular docking analysis, we designed and synthesized 5-((arylfuran/1H-pyrrol-2-yl)methylene)-2-thioxo-3-(3-(trifluoromethyl)phenyl)thiazolidin-4-ones (12a-o) as HIV-1 entry inhibitors. Compounds 12a-o effectively inhibited infection by both laboratory-adapted and primary HIV-1 strains and blocked HIV-1 mediated cell-cell fusion and gp41 six-helix bundle formation. Molecular docking analyses on two highly active inhibitors, 12b, containing a carboxylic acid group, and 12m, containing a tetrazole group, indicated that they both fit snugly into the hydrophobic cavity of HIV-1 gp41 from which each has important ionic interactions with lysine 574 (K574). By contrast, molecular docking of 12i, a less active compound containing a pyrrole instead of a furan ring, indicated a completely different orientation from 12b and 12m and missed critical interactions.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Cell Line
  • Drug Design
  • Furans / chemical synthesis*
  • Furans / chemistry
  • Furans / pharmacology
  • HIV Envelope Protein gp41 / metabolism*
  • HIV Fusion Inhibitors / chemical synthesis*
  • HIV Fusion Inhibitors / chemistry
  • HIV Fusion Inhibitors / pharmacology
  • HIV-1 / drug effects*
  • HIV-1 / isolation & purification
  • HIV-1 / physiology
  • Humans
  • Models, Molecular
  • Pyrroles / chemical synthesis*
  • Pyrroles / chemistry
  • Pyrroles / pharmacology
  • Structure-Activity Relationship
  • Thiazolidines / chemical synthesis*
  • Thiazolidines / chemistry
  • Thiazolidines / pharmacology
  • Virus Internalization

Substances

  • Furans
  • HIV Envelope Protein gp41
  • HIV Fusion Inhibitors
  • Pyrroles
  • Thiazolidines