Influence of adhesive properties on resin-dentin bond strength of one-step self-etching adhesives

J Adhes Dent. 2011 Oct;13(5):417-24. doi: 10.3290/j.jad.a19812.

Abstract

Purpose: To evaluate the association between the resin-dentin bond strength (microtensile bond strength, μTBS) and the physical properties (ultimate tensile strength [UTS] and microhardness [VHN]) of the cured adhesive resin using five commercial one-step self-etching systems.

Materials and methods: Futurabond NR, Go, G Bond, 1-step All Bond SE and Clearfil S3 Bond were applied on flat superficial dentin surfaces. Each adhesive system was applied in five teeth. A resin buildup was then made. After 24 h, resin-dentin beams (0.9 mm2) were prepared to be tested immediately at 0.5 mm/min. For the UTS measurement, hourglass specimens were prepared with each adhesive system (n = 5) to be tested under tensile stress at 0.5 mm/min. The fractured specimens from the UTS test were taken to a Vickers microhardness tester (25 gf/20 s). μTBS, UTS, and VHN values were submitted to a one-way ANOVA and Tukey's test (α = 0.05) for pairwise comparisons. Correlations between μTBS, UTS and VHN were analyzed using the Pearson product moment correlation test (α = 0.05).

Results: Significantly higher μTBS values were observed for 1-step All Bond SE and Clearfil S3 Bond (p > 0.05). The adhesive All Bond SE showed the highest UTSmean among all systems (p < 0.05). The adhesives All Bond SE and G-Bond showed the highest microhardness mean among all systems (p < 0.05). A strong (r = 0.93) and significant (p = 0.021) correlation was only found between the μTBS and UTS values.

Conclusion: The ultimate tensile strength of one-step self-etching systems correlates with the resin-dentin bond strength values.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acid Etching, Dental / methods*
  • Adhesiveness
  • Carbon Compounds, Inorganic / chemistry
  • Composite Resins / chemistry
  • Dental Bonding*
  • Dental Stress Analysis / instrumentation
  • Dentin / ultrastructure*
  • Dentin-Bonding Agents / chemistry*
  • Hardness
  • Humans
  • Humidity
  • Materials Testing
  • Methacrylates / chemistry
  • Resin Cements / chemistry*
  • Silicon Compounds / chemistry
  • Smear Layer
  • Stress, Mechanical
  • Surface Properties
  • Temperature
  • Tensile Strength
  • Time Factors
  • Water / chemistry

Substances

  • All-Bond system
  • Carbon Compounds, Inorganic
  • Charisma composite resin
  • Clearfil S3 Bond
  • Composite Resins
  • Dentin-Bonding Agents
  • G-Bond
  • Go self-etching primer
  • Methacrylates
  • Resin Cements
  • Silicon Compounds
  • futurabond NR
  • Water
  • silicon carbide