Synthesis of enantiopure 2-carba-cyclic phosphatidic acid and effects of its chirality on biological functions

Biochim Biophys Acta. 2011 Apr;1811(4):271-7. doi: 10.1016/j.bbalip.2011.01.003. Epub 2011 Jan 28.

Abstract

Cyclic phosphatidic acid (cPA) is a naturally occurring phospholipid mediator, which has a quite unique cyclic phosphate ring at sn-2 and sn-3 positions of the glycerol backbone. We have designed and chemically synthesized several metabolically stabilized derivatives of cPA. 2-Carba-cPA (2ccPA) is one of the synthesized compounds in which the phosphate oxygen was replaced with a methylene group at the sn-2 position, and it showed much more potent biological activities than natural cPA. Here, we developed a new method of 2ccPA enantiomeric synthesis. And we examined the effects of 2ccPA enantiomers on autotaxin (ATX) activity, cancer cell invasion and nociceptive reflex. As well as racemic-2ccPA, both enantiomers showed inhibitory effects on ATX activity, cancer cell invasion and nociceptive reflex. As their effects were not significantly different from each other, the chirality of 2ccPA may not be critical for these biological functions of 2ccPA.

MeSH terms

  • Animals
  • Breast Neoplasms / drug therapy*
  • Cell Movement / drug effects*
  • Culture Media, Conditioned / pharmacology
  • Female
  • Humans
  • Lysophospholipids / chemistry
  • Male
  • Multienzyme Complexes / antagonists & inhibitors
  • Multienzyme Complexes / metabolism*
  • Phosphatidic Acids / chemical synthesis
  • Phosphatidic Acids / chemistry*
  • Phosphatidic Acids / pharmacology
  • Phosphodiesterase I / antagonists & inhibitors
  • Phosphodiesterase I / metabolism*
  • Phosphoric Diester Hydrolases
  • Pyrophosphatases / antagonists & inhibitors
  • Pyrophosphatases / metabolism*
  • Rats
  • Rats, Wistar
  • Reflex / drug effects*
  • Reflex / physiology
  • Spinal Nerves / drug effects*
  • Spinal Nerves / physiology
  • Tumor Cells, Cultured

Substances

  • 2-carba-cyclic phosphatidic acid
  • Culture Media, Conditioned
  • Lysophospholipids
  • Multienzyme Complexes
  • Phosphatidic Acids
  • Phosphoric Diester Hydrolases
  • Phosphodiesterase I
  • alkylglycerophosphoethanolamine phosphodiesterase
  • Pyrophosphatases