Two copper(II) complexes with 4-benzoylpyridine ligand: synthesis, crystal structure and luminescent properties

Spectrochim Acta A Mol Biomol Spectrosc. 2011 Sep;79(5):1338-44. doi: 10.1016/j.saa.2011.04.065. Epub 2011 May 26.

Abstract

Two new copper(II) complexes Cu(NCS)2(4-Bzpy)2 (1) and Cu(NO3)2(4-Bzpy)4 (2) (4-Bzpy=4-benzoylpyridine) have been synthesized and characterized by IR, UV, elemental analysis and X-ray crystallography. Cu(II) atom has a square planar environment for 1 and an distorted octahedral environment for 2, respectively. In solid state there are C-H⋯π interactions and C-H⋯S hydrogen bonds between adjacent molecules in complex 1. The molecule of complex 2 is further connected by multiform π-π interactions, C-H⋯π interactions and C-H⋯O hydrogen bonds to form a three-dimensional supramolecular structure. The luminescent properties of the complexes 1 and 2 were both investigated in H2O solution and in solid state at room temperature, respectively.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Copper / chemistry*
  • Copper / metabolism*
  • Crystallography, X-Ray
  • Hydrogen Bonding
  • Luminescence
  • Models, Molecular
  • Organometallic Compounds / chemical synthesis*
  • Organometallic Compounds / pharmacology
  • Pyridines / chemistry*
  • Pyridines / metabolism*

Substances

  • Organometallic Compounds
  • Pyridines
  • 4-benzoylpyridine
  • Copper