Quantitative in situ TEM tensile testing of an individual nickel nanowire

Nanotechnology. 2011 Sep 2;22(35):355702. doi: 10.1088/0957-4484/22/35/355702. Epub 2011 Aug 5.

Abstract

In this paper, we have demonstrated the usage of a novel micro-mechanical device (MMD) to perform quantitative in situ tensile tests on individual metallic nanowires inside a transmission electron microscope (TEM). Our preliminary experiment on a 360 nm diameter nickel nanowire showed that the sample fractured at an engineering stress of ∼ 1.2 GPa and an engineering strain of ∼ 4%, which is consistent with earlier experiments performed inside a scanning electron microscope (SEM). With in situ high resolution TEM imaging and diffraction capabilities, this novel experimental set-up could provide unique opportunities to reveal the underlying deformation and damage mechanisms for metals at the nanoscale.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.