RNA-protein binding interface in the telomerase ribonucleoprotein

Proc Natl Acad Sci U S A. 2011 Dec 20;108(51):20333-8. doi: 10.1073/pnas.1100270108. Epub 2011 Nov 28.

Abstract

Telomerase is a specialized reverse transcriptase containing an intrinsic telomerase RNA (TR) which provides the template for telomeric DNA synthesis. Distinct from conventional reverse transcriptases, telomerase has evolved a unique TR-binding domain (TRBD) in the catalytic telomerase reverse transcriptase (TERT) protein, integral for ribonucleoprotein assembly. Two structural elements in the vertebrate TR, the pseudoknot and CR4/5, bind TERT independently and are essential for telomerase enzymatic activity. However, the details of the TR-TERT interaction have remained elusive. In this study, we employed a photoaffinity cross-linking approach to map the CR4/5-TRBD RNA-protein binding interface by identifying RNA and protein residues in close proximity. Photoreactive 5-iodouridines were incorporated into the medaka CR4/5 RNA fragment and UV cross-linked to the medaka TRBD protein fragment. The cross-linking RNA residues were identified by alkaline partial hydrolysis and cross-linked protein residues were identified by mass spectrometry. Three CR4/5 RNA residues (U182, U187, and U205) were found cross-linking to TRBD amino acids Tyr503, Phe355, and Trp477, respectively. This CR4/5 binding pocket is distinct and separate from the previously proposed T pocket in the Tetrahymena TRBD. Based on homologous structural models, our cross-linking data position the essential loop L6.1 adjacent to the TERT C-terminal extension domain. We thus propose that stem-loop 6.1 facilitates proper TERT folding by interacting with both TRBD and C-terminal extension. Revealing the telomerase CR4/5-TRBD binding interface with single-residue resolution provides important insights into telomerase ribonucleoprotein architecture and the function of the essential CR4/5 domain.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Catalysis
  • Cross-Linking Reagents / chemistry
  • Escherichia coli / genetics
  • Humans
  • Kinetics
  • Mass Spectrometry / methods
  • Models, Genetic
  • Models, Molecular
  • Molecular Conformation
  • Nucleic Acid Conformation
  • Peptides / chemistry
  • RNA / chemistry*
  • RNA-Binding Proteins / chemistry*
  • Ribonucleoproteins / chemistry*
  • Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization
  • Telomerase / chemistry*
  • Tetrahymena / metabolism

Substances

  • Cross-Linking Reagents
  • Peptides
  • RNA-Binding Proteins
  • Ribonucleoproteins
  • RNA
  • Telomerase