Quantitative chemical imaging with multiplex stimulated Raman scattering microscopy

J Am Chem Soc. 2012 Feb 29;134(8):3623-6. doi: 10.1021/ja210081h. Epub 2012 Feb 15.

Abstract

Stimulated Raman scattering (SRS) microscopy is a newly developed label-free chemical imaging technique that overcomes the speed limitation of confocal Raman microscopy while avoiding the nonresonant background problem of coherent anti-Stokes Raman scattering (CARS) microscopy. Previous demonstrations have been limited to single Raman band measurements. We present a novel modulation multiplexing approach that allows real-time detection of multiple species using the fast Fourier transform. We demonstrate the quantitative determination of chemical concentrations in a ternary mixture. Furthermore, two imaging applications are pursued: (1) quantitative determination of oil content as well as pigment and protein concentration in microalgae cultures; and (2) 3D high-resolution imaging of blood, lipids, and protein distribution in ex vivo mouse skin tissue. We believe that quantitative multiplex SRS uniquely combines the advantage of fast label-free imaging with the fingerprinting capability of Raman spectroscopy and enables numerous applications in lipid biology as well as biomedical imaging.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Animals
  • Chlorophyta / cytology
  • Lipids / chemistry*
  • Mice
  • Microalgae / chemistry
  • Microalgae / cytology
  • Proteins / chemistry*
  • Skin / chemistry
  • Spectrum Analysis, Raman / instrumentation
  • Spectrum Analysis, Raman / methods*

Substances

  • Lipids
  • Proteins