Biomimetic total synthesis of (-)-isatisine A

Org Lett. 2012 Mar 16;14(6):1624-7. doi: 10.1021/ol300379g. Epub 2012 Feb 28.

Abstract

The biomimetic total synthesis of (-)-isatisine A, a novel alkaloid with an unprecedented fused tetracyclic skeleton, was accomplished in 8 steps from indole and 4,6-O-isopropylidene-protected glucal. The synthesis features a convergent synthetic strategy which relies on nucleophilic addition and a biomimetic benzilic ester rearrangement as key reactions.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Indole Alkaloids / chemical synthesis*
  • Indole Alkaloids / chemistry
  • Isatin / analogs & derivatives*
  • Isatin / chemical synthesis
  • Isatin / chemistry
  • Isatis / chemistry
  • Molecular Structure
  • Plants, Medicinal / chemistry
  • Stereoisomerism

Substances

  • Indole Alkaloids
  • isatisine A
  • Isatin