Comparison of open-flow microperfusion and microdialysis methodologies when sampling topically applied fentanyl and benzoic acid in human dermis ex vivo

Pharm Res. 2012 Jul;29(7):1808-20. doi: 10.1007/s11095-012-0705-9. Epub 2012 Mar 15.

Abstract

Purpose: The purpose of this study is to compare two sampling methods--dermal Open-Flow Microperfusion (dOFM) and dermal Microdialysis (dMD) in an international joint experiment in a single-laboratory setting. We used human ex-vivo skin and sampled topically administered Fentanyl and Benzoic Acid. The second purpose was to provide guidance to researchers in choosing the most efficient method for a given penetrant and give suggestions concerning critical choices for successful dermal sampling.

Methods: The dOFM and dMD techniques are compared in equal set-ups using three probe-types (one dOFM probe and two dMD probe-types) in donor skin (n = 9)--27 probes of each type sampling each penetrant in solutions applied in penetrationchambers glued to the skin surface over a time range of 20 h.

Results: Pharmacokinetic results demonstrated concordance between dOFM and dMD sampling technique under the given experimental conditions. The methods each had advantages and limitations in technical, practical and hands-on comparisons.

Conclusion: When planning a study of cutaneous penetration the advantages and limitations of each probe-type have to be considered in relation to the scientific question posed, the physico-chemical characteristics of the substance of interest, the choice of experimental setting e.g. ex vivo/in vivo and the analytical skills available.

Publication types

  • Comparative Study

MeSH terms

  • Administration, Topical
  • Analgesics, Opioid / administration & dosage
  • Analgesics, Opioid / pharmacokinetics*
  • Benzoic Acid / administration & dosage
  • Benzoic Acid / pharmacokinetics*
  • Dermis / metabolism
  • Equipment Design
  • Female
  • Fentanyl / administration & dosage
  • Fentanyl / pharmacokinetics*
  • Humans
  • Microdialysis / instrumentation
  • Microdialysis / methods*
  • Perfusion / instrumentation
  • Perfusion / methods*
  • Skin Absorption*

Substances

  • Analgesics, Opioid
  • Benzoic Acid
  • Fentanyl