Modulating supramolecular assemblies and mechanical properties of engineered protein materials by fluorinated amino acids

Biomacromolecules. 2012 Aug 13;13(8):2273-8. doi: 10.1021/bm3005116. Epub 2012 Jul 24.

Abstract

Here we describe the biosynthesis and characterization of fluorinated protein block polymers comprised of the two self-assembling domains (SADs): elastin (E) and the coiled-coil region of cartilage oligomeric matrix proteins (C). Fluorination is achieved by residue-specific incorporation of p-fluorophenylalanine (pFF) to create pFF-EC, pFF-CE, and pFF-ECE. Global fluorination results in downstream effects on the temperature-dependent secondary structure, supramolecular assembly, and bulk mechanical properties. The impact of fluorination on material properties also differs depending on the orientation of the block configurations as well as the number of domains in the fusion. These studies suggest that integration of fluorinated amino acids within protein materials can be employed to tune the material properties, especially mechanical integrity.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Amino Acid Substitution
  • Amino Acids / chemistry
  • Elastic Modulus
  • Elastin / biosynthesis
  • Elastin / chemistry*
  • Elastin / genetics
  • Escherichia coli
  • Extracellular Matrix Proteins / biosynthesis
  • Extracellular Matrix Proteins / chemistry*
  • Extracellular Matrix Proteins / genetics
  • Fluorocarbon Polymers / chemistry*
  • Glycoproteins / biosynthesis
  • Glycoproteins / chemistry*
  • Glycoproteins / genetics
  • Matrilin Proteins
  • Molecular Sequence Data
  • Phenylalanine / chemistry*
  • Protein Engineering
  • Protein Structure, Quaternary
  • Protein Structure, Secondary
  • Rheology
  • Sequence Analysis, Protein
  • Transition Temperature
  • Viscosity

Substances

  • Amino Acids
  • Extracellular Matrix Proteins
  • Fluorocarbon Polymers
  • Glycoproteins
  • Matrilin Proteins
  • Phenylalanine
  • Elastin