Withaferin A binds covalently to the N-terminal domain of annexin A2

Biol Chem. 2012 Oct;393(10):1151-63. doi: 10.1515/hsz-2012-0184.

Abstract

Annexin A2 (AnxA2), a 38-kDa member of the Ca2+-binding annexin family, has been implicated in numerous cancer pathways. Withaferin A (WithfA), a natural plant compound, has been reported previously to bind covalently to Cys133 of the AnxA2 core domain leading to a reduction of the invasive capabilities of cancer cells by altering their cytoskeleton. We show here that AnxA2 has an inhibitory effect on actin polymerization, and a modification with WithfA significantly increases this inhibitory role of AnxA2. Using mass spectrometry and single-site mutants, we localized the WithfA-AnxA2 interaction to the N-terminal domain of AnxA2 where WithfA binds covalently to Cys9. Whereas binding to F-actin filaments has been mapped to the C terminus of AnxA2, our results suggest that the N-terminal domain modified by WithfA may also play a role in the AnxA2-actin interaction. The binding of WithfA may regulate the AnxA2-mediated actin dynamics in two distinct ways: (i) the increase of F-actin bundling activity by the Anx2/p11 heterotetramer and (ii) the decrease of actin polymerization as a result of the increased affinity of AnxA2 to the barbed end of actin microfilaments. We demonstrate the susceptibility of Cys9 of AnxA2 to chemical modifications and exclude Cys133 as a binding site for WithfA.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Actins / chemistry
  • Animals
  • Annexin A2 / chemistry*
  • Annexin A2 / metabolism*
  • Annexin A2 / pharmacology
  • Binding Sites
  • Cattle
  • Cysteine / metabolism
  • Humans
  • Models, Molecular
  • Protein Binding
  • Protein Multimerization / drug effects
  • Protein Structure, Quaternary
  • Protein Structure, Tertiary
  • Solvents / chemistry
  • Withanolides / metabolism*

Substances

  • Actins
  • Annexin A2
  • Solvents
  • Withanolides
  • Cysteine
  • withaferin A