A novel pH sensitive water soluble fluorescent nanomicellar sensor for potential biomedical applications

Bioorg Med Chem. 2013 Nov 1;21(21):6292-302. doi: 10.1016/j.bmc.2013.08.064. Epub 2013 Sep 11.

Abstract

Herein we report on the synthesis and sensor activity of a novel pH sensitive probe designed as highly water-soluble fluorescent micelles by grafting of 1,8-naphthalimide-rhodamine bichromophoric FRET system (RNI) to the PMMA block of a well-defined amphiphilic diblock copolymer-poly(methyl methacrylate)-b-poly(methacrylic acid) (PMMA48-b-PMAA27). The RNI-PMMA48-b-PMAA27 adduct is capable of self-assembling into micelles with a hydrophobic PMMA core, containing the anchored fluorescent probe, and a hydrophilic shell composed of PMAA block. Novel fluorescent micelles are able to serve as a highly sensitive pH probe in water and to internalize successfully HeLa and HEK cells. Furthermore, they showed cell specificity and significantly higher photostability than that of a pure organic dye label such as BODIPY. The valuable properties of the newly prepared fluorescent micelles indicate the high potential of the probe for future biological and biomedical applications.

Keywords: 1,8-Naphthalimide/rhodamine 6G bichromophore; Fluorescent micelles; Fluorescent resonance energy transfer (FRET); Living cells; Well-defined PMMA–PMAA block copolymer; pH sensor.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cell Survival / drug effects
  • Fluorescence Resonance Energy Transfer
  • Fluorescent Dyes / chemical synthesis
  • Fluorescent Dyes / chemistry*
  • Fluorescent Dyes / toxicity
  • HEK293 Cells
  • HeLa Cells
  • Humans
  • Hydrogen-Ion Concentration
  • Hydrophobic and Hydrophilic Interactions
  • Micelles*
  • Nanoparticles / chemistry*
  • Naphthalimides / chemical synthesis
  • Naphthalimides / chemistry
  • Polymethacrylic Acids / chemical synthesis
  • Polymethacrylic Acids / chemistry
  • Polymethacrylic Acids / toxicity
  • Rhodamines / chemical synthesis
  • Rhodamines / chemistry
  • Water / chemistry

Substances

  • Fluorescent Dyes
  • Micelles
  • Naphthalimides
  • Polymethacrylic Acids
  • Rhodamines
  • rhodamine 6G
  • Water
  • methylmethacrylate-methacrylic acid copolymer