Gene cloning, expression and characterisation of a new β-agarase, AgWH50C, producing neoagarobiose from Agarivorans gilvus WH0801

World J Microbiol Biotechnol. 2014 Jun;30(6):1691-8. doi: 10.1007/s11274-013-1591-y. Epub 2014 Jan 7.

Abstract

agWH50C, a novel β-agarase gene, was cloned from Agarivorans gilvus WH0801 by degenerate PCR and nested PCR. The gene agWH50C comprized a 2,223-bp, encoding a protein of 740 amino acids. Sequencing results demonstrated that AgWH50C shared 45 % sequence identity with a well characterized β-agarase, Aga50D, from Saccharophagus degradans 2-40. The mature agarase was expressed in Escherichia coli and purified by affinity chromatography. The optimum pH and temperature for AgWH50C activity were 6.0 and 30 °C. The K m and V max values for agarose were 12.55 mg/ml and 1.17 U/mg. Analysis of the hydrolysis products using linear ion trap mass spectrometry, Fourier transform-nuclear magnetic resonance spectrometry and thin-layer chromatography confirmed that the reaction product of AgWH50c was α-neoagarobiose alone. Therefore, our novel agarase has the potential for industrial applications to produce neoagarobiose as well as provides a key β-agarase for fermentation of agar biomass.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alteromonadaceae / chemistry
  • Alteromonadaceae / enzymology*
  • Alteromonadaceae / genetics
  • Amino Acid Sequence
  • Bacterial Proteins / chemistry*
  • Bacterial Proteins / genetics
  • Bacterial Proteins / metabolism
  • Cloning, Molecular*
  • Disaccharides / metabolism*
  • Enzyme Stability
  • Gene Expression
  • Glycoside Hydrolases / chemistry*
  • Glycoside Hydrolases / genetics
  • Glycoside Hydrolases / metabolism
  • Hydrogen-Ion Concentration
  • Kinetics
  • Molecular Sequence Data
  • Sequence Alignment

Substances

  • Bacterial Proteins
  • Disaccharides
  • neoagarobiose
  • Glycoside Hydrolases
  • agarase

Associated data

  • GENBANK/KC913197