Optimization and validation of a neutralizing antibody assay for HIV-1 in A3R5 cells

J Immunol Methods. 2014 Jul:409:147-60. doi: 10.1016/j.jim.2014.02.013. Epub 2014 Mar 6.

Abstract

A3R5 is a human CD4(+) lymphoblastoid cell line that was engineered to express CCR5 and is useful for the detection of weak neutralizing antibody responses against tier 2 strains of HIV-1. Here we describe the optimization and validation of the HIV-1 neutralizing antibody assay that utilizes A3R5 cells, performed in compliance with Good Clinical Laboratory Practice (GCLP) guidelines. The assay utilizes Renilla luciferase-expressing replication competent infectious molecular clones (IMC) encoding heterologous env genes from different HIV-1 clades. Key assay validation parameters tested included specificity, accuracy, precision, limit of detection and quantitation, specificity, linearity and range, and robustness. Plasma samples demonstrated higher non-specific activity than serum samples in the A3R5 assay. This assay can tolerate a wide range of virus input but is more sensitive to cell concentration. The higher sensitivity of the A3R5 assay in neutralization responses to tier 2 strains of HIV-1 makes it complementary to, but not a substitute for the TZM-bl assay. The validated A3R5 assay is employed as an endpoint immunogenicity test for vaccine-elicited neutralizing antibodies against tier 2 strains of HIV-1, and to identify correlates of protection in HIV-1 vaccine trials conducted globally.

Keywords: A3R5 cells; Assay validation; HIV; Neutralizing antibody.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't
  • Validation Study

MeSH terms

  • Antibodies, Neutralizing / blood*
  • Automation, Laboratory / standards
  • Biomarkers / blood
  • Cell Line
  • Guideline Adherence / standards
  • HIV Antibodies / blood*
  • HIV Infections / blood
  • HIV Infections / diagnosis*
  • HIV Infections / immunology
  • HIV-1 / genetics
  • HIV-1 / immunology*
  • High-Throughput Screening Assays / standards*
  • Humans
  • Limit of Detection
  • Neutralization Tests / standards*
  • Observer Variation
  • Practice Guidelines as Topic / standards
  • Predictive Value of Tests
  • Quality Control
  • Reproducibility of Results
  • Time Factors
  • Transfection

Substances

  • Antibodies, Neutralizing
  • Biomarkers
  • HIV Antibodies