Rapid synthesis of water-dispersible superparamagnetic iron oxide nanoparticles by a microwave-assisted route for safe labeling of endothelial progenitor cells

Acta Biomater. 2014 Aug;10(8):3775-85. doi: 10.1016/j.actbio.2014.04.010. Epub 2014 Apr 20.

Abstract

We synthesize highly crystalline citrate-coated iron oxide superparamagnetic nanoparticles that are stable and readily dispersible in water by an extremely fast microwave-assisted route and investigate the uptake of magnetic nanoparticles by endothelial cells. Nanoparticles form large aggregates when added to complete endothelial cell medium. The size of the aggregates was controlled by adjusting the ionic strength of the medium. The internalization of nanoparticles into endothelial cells was then investigated by transmission electron microscopy, magnetometry and chemical analysis, together with cell viability assays. Interestingly, a sevenfold more efficient uptake was found for systems with larger nanoparticle aggregates, which also showed significantly higher magnetic resonance imaging effectiveness without compromising cell viability and functionality. We are thus presenting an example of a straightforward microwave synthesis of citrate-coated iron oxide nanoparticles for safe endothelial progenitor cell labeling and good magnetic resonance cell imaging with potential application for magnetic cell guidance and in vivo cell tracking.

Keywords: Cellular uptake; Endothelial progenitor cells; Iron oxide nanoparticles; Magnetic resonance imaging; Microwave synthesis.

Publication types

  • Research Support, Non-U.S. Gov't
  • Retracted Publication

MeSH terms

  • Animals
  • Cell Tracking / methods*
  • Citric Acid / chemistry
  • Contrast Media / chemistry
  • Dextrans / chemistry*
  • Diffusion
  • Drug Compounding / methods
  • Endothelial Cells
  • Endothelial Progenitor Cells / chemistry*
  • Endothelial Progenitor Cells / cytology*
  • Humans
  • Magnetic Resonance Imaging / methods*
  • Magnetite Nanoparticles / chemistry*
  • Male
  • Mice
  • Mice, Inbred BALB C
  • Microwaves
  • Particle Size
  • Staining and Labeling / methods
  • Water / chemistry*

Substances

  • Contrast Media
  • Dextrans
  • Magnetite Nanoparticles
  • ferumoxtran-10
  • Water
  • Citric Acid