An efficient tandem approach for the synthesis of functionalized 2-pyridone-3-carboxylic acids using three-component reaction in aqueous media

Mol Divers. 2014 Aug;18(3):535-43. doi: 10.1007/s11030-014-9522-x. Epub 2014 May 4.

Abstract

Novel analogs of 2-pyridone-3-carboxylic acids 4a-l have been prepared by the three-component reaction of 3-formyl chromone, Meldrum's acid, and primary amines in the presence of a catalytic amount of diammonium hydrogen phosphate in water. Good-to-high yields, easy work-up, and an environmentally friendly profile are the advantages of this method for the synthesis of 2-pyridone-3-carboxylic acid derivatives.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amines / chemistry
  • Carboxylic Acids / chemical synthesis*
  • Carboxylic Acids / chemistry*
  • Chemistry Techniques, Synthetic
  • Phosphates / chemistry
  • Water / chemistry*

Substances

  • Amines
  • Carboxylic Acids
  • Phosphates
  • ammonium phosphate
  • Water